With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.13395-16-9,Bis(acetylacetone)copper,as a common compound, the synthetic route is as follows.
Under a nitrogen atmosphere, copper acetylacetonate (0.9 mmol) was dissolved in 25 mL of dichloromethane, followed by addition of 1,10-phenanthroline (0.9 mmol). The reaction solution was stirred at room temperature for 48 hours and then concentrated in vacuo. The resulting solid was washed with 25 mL of n-pentane and recrystallized with dichloromethane and n-pentane to obtain Catalyst 3. The method of the invention produces this compound in a yield of up to 75%
The synthetic route of 13395-16-9 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Chinese Academy Of Sciences Lanzhou Chemical Physics Institute Suzhou Institute; Li Yuehui; Wang Hua; Dong Yanan; Ke Lisitian¡¤shanduofu; (20 pag.)CN108017557; (2018); A;,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”