Bis(acetylacetone)copper, cas is 13395-16-9, it is a common heterocyclic compound, the copper-catalyst compound, its synthesis route is as follows.
A yellow solution of H4L (0.30mmol, 0.068g) in dmf (6mL) was added to a turquoise solution of Cu(acac)2 (0.30mmol, 0.079g) in dmf (20mL). The immediately formed green solution was refluxed for 3h and left for slow evaporation. X-ray quality blue crystals of 3¡¤1.5dmf were formed after 2months, which were filtered off and dried under vacuum. (Yield: 0.053g, ?60%). The solid was analyzed as solvent free. C44H56Cu4N4O18 requires: C, 44.67; H, 4.77; N, 4.73%. Found: C, 44.49; H, 4.74; N, 4.70. FT-IR (KBr pellets, cm-1): 3553(s), 3477(s), 3414(s), 1638(s), 1617(vs), 1578(s), 1553(s), 1533(s), 1462(w), 1413(m), 1384(m), 1355(s), 1275(s), 1189(s), 1020(s), 937(s), 782(s), 684(m), 653(w), 613(s), 480(m), 455(s).
With the rapid development of chemical substances, we look forward to future research findings about 13395-16-9
Reference£º
Article; Lazarou, Katerina N.; Savvidou, Aikaterini; Raptopoulou, Catherine P.; Psycharis, Vassilis; Polyhedron; vol. 152; (2018); p. 125 – 137;,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”