Name is Copper(II) trifluoromethanesulfonate, as a common heterocyclic compound, it belongs to copper-catalyst compound, and cas is 34946-82-2, its synthesis route is as follows.
Copper(II) triflate (50.0 mg, 0.14 mmol) was dissolved in methanol (3 ml) and the ligand (42.8 mg, 0.07 mmol) added. The reaction mixture was stirred at r. t. for 16 h. Then the mixture was evaporated to dryness and the resulting green solid recrystallised from dichloromethane and pentane. 5: 23.6 mg, 34.0%. C42H37N5O8S2F6Cu¡¤2CH2Cl2: Anal. Calc. C, 43.16; H, 3.30; N, 5.59. Found: C, 42.72; H, 3.71; N, 5.87%. HR-MS: C40H36N5O263Cu Calc. 681.2239. Found: 681.2202 (100.0), C40H36N5O265Cu Calc. 683.2147. Found 683.2105 (65.1). IR: nunu [cm-1]=3066, 2962, 2870, 1657, 1598, 1535, 1484, 1454, 1265, 1172, 1109, 1032, 953, 756, 639. Magnetic susceptibility in CD2Cl2 (295 K): mueff=1.78muB.
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Reference£º
Article; Sauer, Desiree C.; Wadepohl, Hubert; Polyhedron; vol. 81; (2014); p. 180 – 187;,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”