As a common heterocyclic compound, it belongs to copper-catalyst compound, name is Copper(II) acetate, and cas is 142-71-2, its synthesis route is as follows.
A mixture of 0.04 g (0.065 mmol) of porphin 1 and 0.118 g (0.65 mmol) of Cu(OAc)2 in 40 mL of dimethylformamide was heated under reflux for 15 s. The reaction mixture was cooled, water and solid NaCl was added, the precipitate was separated by filtration, washed with water, dried, and chromatographed on aluminum oxide using chloroform as an eluent to give 0.038 g (0.0562 mmol) (86%) of compound 5. MS (m/z (Irel, %)): 675 (97) [M]+; for C44H28N4Cu calcd.: 676. IR (nu, cm-1): 2926 s, 2855 m nu(C-H, Ph), 1694 w,1598 m 1489 s nu(C=C, Ph), 1441 m nu(C=N), 1371 m, 1346 s nu(C-N), 1146 s, 1071 s delta(C-H, Ph), 1005 s nu(C-C), 861 m, 794 m gamma(C-H, pyrrole ring), 742 m, 696 m gamma(C-H, h), 480 nu(Cu-N).
142-71-2, In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles.,142-71-2 ,Copper(II) acetate, other downstream synthetic routes, hurry up and to see
Reference£º
Article; Chizhova; Shinkarenko; Zav?yalov; Mamardashvili, N. Zh.; Russian Journal of Inorganic Chemistry; vol. 63; 6; (2018); p. 732 – 735; Zh. Neorg. Khim.; vol. 63; 6; (2018); p. 695 – 699,5;,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”