Brief introduction of 34946-82-2

34946-82-2 Copper(II) trifluoromethanesulfonate 2734996, acopper-catalyst compound, is more and more widely used in various.

With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.34946-82-2,Copper(II) trifluoromethanesulfonate,as a common compound, the synthetic route is as follows.

L (0.0424 g, 0.2 mmol), Cu (CF3SO3)2(0.0691g,0.2mmol)H2O (6 mL), CH3CN (4 mL), water and heat 100Oslow C down to room temperature after three days.After opening the autoclave there for X- ray diffraction analysis of the yellow rod-like crystals.Yield: 35%

34946-82-2 Copper(II) trifluoromethanesulfonate 2734996, acopper-catalyst compound, is more and more widely used in various.

Reference£º
Patent; Tianjin Normal University; Wang, Ying; (10 pag.)CN104557986; (2016); B;,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”

Analyzing the synthesis route of 34946-82-2

34946-82-2 Copper(II) trifluoromethanesulfonate 2734996, acopper-catalyst compound, is more and more widely used in various.

34946-82-2, Copper(II) trifluoromethanesulfonate is a copper-catalyst compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

Copper(II) trifluoromethanesulfonate (5 g, 14 mmol) was dissolved in methanol (25 mL). Pyridine(12 mL, 149 mmol) was added dropwise (exothermic reaction was observed) and the reaction mixturewas stirred for 30 min. The mixture was left at ambient temperature for 1 h and thereafter in fridge (at5 C) overnight. The blue crystalline precipitate was filtered off, recrystallized from 20% Py in MeOHand dried under a stream of air affording the desired product [56]. Yield 8.5 g, 91%Appearance blue solidMolecular formula C22H20CuF6N4O6S2Molar mass 678.08042Anal.Calcd for C22H20CuF6N4O6S2: C, 38.97; H, 2.97; N, 8.26. Found: C,39.1 < 0.1; H, 3.16 0.09; N, 8.33 0.01. 34946-82-2 Copper(II) trifluoromethanesulfonate 2734996, acopper-catalyst compound, is more and more widely used in various. Reference£º
Article; Zarrad, Fadi; Zlatopolskiy, Boris D.; Krapf, Philipp; Zischler, Johannes; Neumaier, Bernd; Molecules; vol. 22; 12; (2017);,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”