Category: 6046-93-1

With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.6046-93-1,Copper(II) acetate hydrate,as a common compound, the synthetic route is as follows.

meso-Tetraphenylporphyrin (TPP)(2 g, 3.25 mmol) was dissolved in CH2Cl2 (160 mL) and methanol (50 mL). Cu(OAc)2¡¤H2O (1.2 g,5.85 mmol) was added and the mixture was heated to reflux for 2 h until all starting material wasconsumed (TLC, UV-vis). Solvents were evaporated to give a red-purple residue that was filteredthrough a short plug of silica. After filtration, the product 3 was obtained as a dark purple sparklingsolid (2.2 g, 3.25 mmol, 99%)

As the paragraph descriping shows that 6046-93-1 is playing an increasingly important role.

Reference£º
Article; Blom, Magnus; Norrehed, Sara; Andersson, Claes-Henrik; Huang, Hao; Light, Mark E.; Bergquist, Jonas; Grennberg, Helena; Gogoll, Adolf; Molecules; vol. 21; 1; (2016);,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”

6046-93-1, Copper(II) acetate hydrate is a copper-catalyst compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

General procedure: A solution of Cu(OAc)2¡¤H2O (4.6 mmol) in methanol (10 mL) was added to a solution of corresponding porphyrin (1.15 mmol) in methylene chloride (50 mL). The resulting mixture was stirred flor 1.5 h at room temperature with TLC monitoring (CHCl3-hexane 1:2). Then the reaction mixture was poured into water and extracted with methylene chloride. The organic layer was dried over Na2SO4, and the solvent was removed under reduced pressure. The residue was used without purification. 5,10,15,20-(tetraphenylporphyrinato)copper(II) (13) [56] (757 mg,yield 97%). UV-Vis (CH2Cl2) >max, (j10-3) nm: 414 (611), 539 (29).APCI-MS Found: [M]+ 676.16; ?C44H28CuN4? requires [M]+ 676.26.

As the paragraph descriping shows that 6046-93-1 is playing an increasingly important role.

Reference£º
Article; Ol’shevskaya, Valentina A.; Alpatova, Viktoriya M.; Radchenko, Alexandra S.; Ramonova, Alla A.; Petrova, Albina S.; Tatarskiy, Victor V.; Zaitsev, Andrei V.; Kononova, Elena G.; Ikonnikov, Nikolay S.; Kostyukov, Alexey A.; Egorov, Anton E.; Moisenovich, Mikhail M.; Kuzmin, Vladimir A.; Bragina, Natalya A.; Shtil, Alexander A.; Dyes and Pigments; vol. 171; (2019);,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”