Downstream synthetic route of Copper(I) bromide

With the synthetic route has been constantly updated, we look forward to future research findings about Copper(I) bromide,belong copper-catalyst compound

As a common heterocyclic compound, it belongs to quinuclidine compound,Quinuclidine-4-carboxylic acid hydrochloride,40117-63-3,Molecular formula: C8H14ClNO365,mainly used in chemical industry, its synthesis route is as follows.,7787-70-4

A solution of (4-diphenylphosphino)phenanthridine (0.023 g,0.063 mmol) in CH2Cl2 (3 mL) was added drop-wise to a suspensionof CuBr (0.089 g, 0.063 mmol) in CH2Cl2 (3 mL) with constantstirring. The reaction mixture was stirred for overnight at roomtemperature. Then the reaction mixture was filtered through smallplug of Celite and dried under vacuum to give an orange solid.Yield = 0.022 g (71%).

With the synthetic route has been constantly updated, we look forward to future research findings about Copper(I) bromide,belong copper-catalyst compound

Reference£º
Article; Mondal, Rajarshi; Giesbrecht, Patrick K.; Herbert, David E.; Polyhedron; vol. 108; (2016); p. 156 – 162;,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”